CHEMISTRY 221L
QUANTITATIVE ANALYSIS LABORATORY
Laboratory Schedule —
Spring 2007
Text: Exploring Chemical Analysis, Daniel C. Harris
| Dr. Julian McGill | Tuesday Laboratory | Room 303 |
| Dr. W. Frank Kinard | Wednesday Laboratory | Room 310 |
| Dr. Gary Asleson | Thursday Laboratory | Room 307 |
| Lab Days | Week | Laboratory Reading Assignments | Reference | Results Due |
| January 9, 2007 | 1 |
CHECK-IN —
Safety Orientation Analytical Balance Operation Introduction to Statistics Introduction to Computer Use |
Exp. 21-1 (383) | January 16, 2007 |
| January 10, 2007 | Exp. 21-3 (388) | January 17, 2007 | ||
| January 11, 2007 | Handout | January 18, 2007 | ||
| January 16, 2007 | 2 |
Gravimetric Determination of
Calcium as Calcium Oxalate Hydrate |
Exp. 21-4 (389) | January 23, 2007 |
| January 17, 2007 | Handout | January 24, 2007 | ||
| January 18, 2007 | January 25, 2007 | |||
| January 23, 2007 | 3 |
Determination of Calcium by
Titration with EDTA |
Exp. 21-10 (395) | January 30, 2007 |
| January 24, 2007 | January 31, 2007 | |||
| January 25, 2007 | February 1, 2007 | |||
| January 30, 2007 | 4 |
Titrimetric Determination of
Sodium Carbonate |
Exp. 21-6 (391) | February 6, 2007 |
| January 31, 2007 | Exp. 21-7 (392) | February 7, 2007 | ||
| February 1, 2007 | Handout | February 8, 2007 | ||
| February 6, 2007 | 5 |
Determination of the
Equivalent Weight of a Salt by Ion Exchange |
Exp. 21-18 (405) | February 13, 2007 |
| February 7, 2007 | Handout | February 14, 2007 | ||
| February 8, 2007 | February 15, 2007 | |||
| February 13, 2007 | 6 |
Determination of the Formula
Weight and Ionization Constant of an Organic Acid |
Exp. 21-9 (394) | February 20, 2007 |
| February 14, 2007 | Handout | February 21 2007 | ||
| February 15, 2007 | February 22, 2007 | |||
| February 20, 2007 | 7 | Iodometric Determination of Copper | Exp. 21-12 (398) | February 27, 2007 |
| February 21 2007 | Handout | February 28 2007 | ||
| February 22, 2007 | March 1, 2007 | |||
| February 27, 2007 | 8 |
Determination of Ascorbic
Acid in Vitamin C |
Exp. 21-12 (398) | March 13, 2007 |
| February 28 2007 | Handout | March 14, 2007 | ||
| March 1, 2007 | March 15, 2007 | |||
| March 6, 2007 | 9 |
SPRING BREAK |
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| March 7, 2007 | ||||
| March 8, 2007 | ||||
| March 13, 2007 | 10 | Permanganimetric Determination of Iron | Exp. 21-11 (397) | March 20, 2007 |
| March 14, 2007 | Handout | March 21, 2007 | ||
| March 15, 2007 | March 22, 2007 | |||
| March 20, 2007 | 11 |
Spectrophotometric
Determination of Iron as the o-Phenanthroline Complex |
Exp. 21-16 (402) | March 27, 2007 |
| March 21, 2007 | Handout | March 28, 2007 | ||
| March 22, 2007 | March 29, 2007 | |||
| March 27, 2007 | 12 |
Metal Determination by
Atomic Absorption Spectrophotometry |
Handout | April 3, 2007 |
| March 28, 2007 | April 4, 2007 | |||
| March 29, 2007 | April 5, 2007 | |||
| April 3, 2007 | 13 |
Separation and Quantitation
of an Organic Mixture by Gas Chromatography |
Exp. 21-19 (405) | April 10, 2007 |
| April 4, 2007 | Handout | April 11, 2007 | ||
| April 5, 2007 | April 12, 2007 | |||
| April 10, 2007 | 14 | Laboratory Final Exam — CHECK OUT | ||
| April 11, 2007 | ||||
| April 12, 2007 | ||||